Recorder gain set too low. Column overloaded. Sample-column interaction. Detector and/or recorder time constants are set too high. Reduce sample volume and/or concentration. Adjust gain. Inject smaller volume (e.g., 10 μL vs. 100 μL) or 1:10 or 1:100 dilution of sample. Change buffer strength, pH, or mobile phase composition.
Recovery collection with the Aijiren Series purification system. 12-position/13-port valve. 12 recovery locations. simple recovery location tracking by software. Third-party fraction collector and BCD board. Number of recovery locations depend on fraction collector. no recovery location tracking by software.
Aijiren Technology Alliance Total Recovery Vial Specifically designed for the side draw-port needle and the factory needle draw depth settings of the Aijiren Technology Alliance 2690/2695 HPLC. This vial delivers maximum sample capacity (~1 mL) with minimum residual volume (~9 μL). Aijiren Technology Maximum Recovery Vial Specifically designed for the bottom draw-port
Feb 28, 2022 · Dead volume contributes a portion of this volume. Dwell volume – a.k.a gradient delay volume, is the volume from the point of mobile phase mixing to the inlet of the column. HPLC method transfer Now we can take these definitions and start to think about when each term is important. HPLC Dead Volume
Dec 21, 2021 · Low-volume samples. Total Recovery Vials. 12x32mm Vial with Low Volume Inserts. Sample Vials & Accessories Chapter from current catalog. On-line Vials Part Number Selector Tool.
Filtration of acetonitrile using 0.2 µM filters. The smallest volume of acetonitrile that could be consistently filtered was 300 µL. When filtering 100 or 200 µL of acetonitrile sample, the vacuum pressure caused the solvent to spray into the system, which resulted in the sample spilling outside the vial.
Ultra-low Carryover. The Nexera boasts ultra-low carryover, even on a high-sensitivity LC/MS/MS. This reduces time spent on rinsing, resulting in a shorter overall analysis time. Elimination of Dead Volume (Patent Pending) Dead volume in the flow line will lead to carryover from sample residue.
Aug 1, 2019 · autosamplers operate with the sampling needle as part of. the sample loop. It has two major instrumental setups—. with the metering device as part of the high-pressure flow. path (Figure 4a) or
Deactivated Clear Glass 12 x 32 mm Screw Neck Vial with Cap and Preslit PTFE/Silicone Septum, 2 mL Volume, 100/pk. This item is not available for sale. Contact Aijiren Technology for more information. SKU: 186000327C. LCGC Certified Clear Glass 12 x 32 mm Screw Neck Vial, Max Recovery, with Cap and Preslit PTFE/Silicone Septum, 1.5 mL Volume, 100/pk.
Level 3 - vial, cap, and septa kits. EPA Certified Screw Vial & Cap Kits. HPLC & GC Certified Screw Vial & Cap Kits for 2 mL Samples. Precleaned, EPA certified assembled kits; includes 40 mL screw vials and 24 mm. open top screw caps. 0.3 and 1.5 mL screw top vial-cap kits for analysis of small sample volumes.
Sample cooling: Yes, 4-40 °C Depends on sampler selected: Sample capacity (standard) Based on standard 12 mm OD vials (≤ 1.5 mL) 4 racks of 54 vials (≤ 1.5mL) each, other rack formats available + capacity of 12 x 22.5 mm OD vials (≤ 10 mL) in the carousel: Sampler extension available: Yes, with Vanquish Charger: Column compartment
Chromatography Vials. With thousands of combinations to choose from, DWK Life Sciences offers the largest and most diverse selection of chromatography lab vial solutions and microplates. Our ISO 9001 facility manufactures vials that meet or exceed OEM specifications for headspace, routine HPLC/GC use, plus Certified vials for LCMS/GCMS.
May 12, 2023 · o Larger proteins require less sample than smaller proteins. o Typical range 5 – 500 µg/injection § BSA (67 KDa) 100 µl at 2 mg/ml always gives a good light scattering signal • Sample volume: o Maximum injection volume: 100 µl o Minimum injection volume: 5 µl o Glass autosampler vial with low volume insert has 10 µl dead volume.
High-recovery vials enable sample concentration and injection without transferring to microvolume inserts; Micro-sampling vials offer a lower cost alternative to high-recovery vials; Conical inserts with polymer feet virtually eliminate dead volume and act as a shock absorber for needles; Flat bottom inserts are fitted to vial dimensions
Micro insert vials, when used in conjunction with autosampler vials, allow for maximum sample recovery and easier sample removal because the conical shape decreases the surface area inside the vial.Micro insert vials can be used with screw tops, crimp tops, or snap top vials. All conical styles of inserts are offered with the traditional pulled